Crystal Research and Technology
Cryst. Res. Technol. 34 (1999) 167 - Abstract -

D. Tscheuschner, L. Ratke
German Aerospace Center, DLR, Institute for Space-Simulation, Cologne, Germany

Crystallization of InSb in Aerogel Crucibles

A novel type of a furnace for Vertical-Gradient-Freeze growth VGF of semiconductors is introduced. The basic element - a silica aerogel crucible - allows us to detect the crystallisation front with a suitable IR-CCD-camera due to its transparency. The growth velocity and the temperature gradient ahead of the solid-liquid interface are directly obtained in an optical way from the experiment. This is demonstrated for the growth of InSb. The excellent thermal insulation properties of the aerogels lead to a nearly one-dimensional temperature field and a nearly planar crystallisation front.

Keywords: silica aerogels, VGF, optical detection of the solid/liquid front, one-dimensional temperature field, compound semiconductor InSb, numerical simulation


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