Synthesis and X-ray crystal structure investigations of the complexes of a proton sponge with selected inorganic acids: Crystal structure of DMAN.HI complex by W. Lasocha and A. Rafalska-Lasocha

Crystal Research and Technology

Cryst. Res. Technol. 41, 588 (2006) - Abstract -

Synthesis and X-ray crystal structure investigations of the complexes of a proton sponge with selected inorganic acids: Crystal structure of DMAN.HI complex

W. Lasocha and A. Rafalska-Lasocha

Faculty of Chemistry, Jagiellonian University, 30-060 Krakow, ul. Ingardena 3, Poland

Keywords	X-ray powder diffraction, structure solution, proton sponge complexes
PACS	61.10.Nz
DOI	10.1002/crat.200510630

A series of ionic complexes of 1,8 –bis(dimethylamino)naphthalene with selected inorganic acids such as HCl, HBr, HI, HSCN and HBF₄ were synthesised and thoroughly investigated by means of powder diffractometry and analytical methods. The crystallographic data for these compounds as well as the results of the structure solution by powder diffraction methods of the 1,8 –bis(dimethylamino)naphthalene.HI complex, which crystallizes in the monoclinic system, S.G. P2₁/c (14), a=7.999(2)Å, b=23.053(3)Å, c=7.948(1)Å, β = 99.63°, R_Fwp

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